Nuclear magnetic resonance (NMR) spectroscopy Bruker Avance II+ HD 600 MHz

Bruker Avance II+ 600 console with a Bruker 600 UltraShield^TM magnet and a CentOS workstation with Bruker TopSpin 3.6.5 software. The spectrometer is standard equipped with a 5 mm PABBO BB (³¹P-¹⁰⁹Ag)-1H/D probe with z-gradients and ATM accessory for Automatic Tuning and Matching. The following probes are also available:

• 10 mm PABBO BB (³¹P-¹⁰⁹Ag)-1H/D probe with z-gradients and ATM accessory for Automatic Tuning and Matching
• 10 mm PABBO BBLR (⁴¹K-¹⁰⁹Ag)-1H/D custom probe with z-gradients and ATM accessory for Automatic Tuning and Matching. BB range shifted upwards as to include ⁹⁷Mo, ⁸⁹Y and ¹⁸³W.
• 5 mm SEF 19F-1H/D probe, optimized for ¹⁹F observation with ¹H decoupling.
• 1 mm PATXI 1H/D-13C/15N probe with z-gradients and ATM accessory for Automatic Tuning and Matching
• 5 mm PATXI 600S3 H-C/N-D probe with z-gradients and ATM accessory for Automatic Tuning and Matching
• 5 mm PABBI 1H/D-BB (³¹P-¹⁰⁹Ag) probe with z-gradients and ATM accessory for Automatic Tuning and Matching
• 5 mm SEX 13C-1H/D probe, optimized for temperature ranges of -150 °C to 600 °C
• 4 mm HRMAS 1H/13C/15N/2H probe with ¹H/¹³C/¹⁵N observe or decoupling channels and Magic Angle-gradient

The spectrometer is equipped with a 24-positions sample changer and Bruker Autocalibrate function. The spectrometer runs in Icon-NMR Automation mode.