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Nuclear magnetic resonance (NMR) spectroscopy

(1) Bruker Avance 300 MHz spectrometer: 1H, 13C 1D NMR, lab 00.422

(2) Bruker Avance III HD 400 spectrometer:  1H, 7Li, 11B, 13C, 19F, 27Al, 29Si, 31P, 51V 1D NMR, 1H–1H and 1H–13C 2D NMR, lab 00.422

(3) Bruker Avance II+ HD 600 MHz spectrometer: all NMR-sensitive nuclei, lab 00.421

The NMR Core facilities comprise a high-throughput area intended for daily use (Bruker Advance 300 and Bruker Avance III HD 400 spectrometer) and a research area, dedicated to specialized NMR experiments (Bruker Avance II+ 600 spectrometer).

 

Specifications:

 

  • Bruker Avance 300 console: Bruker 300 UltraShieldTM magnet, equipped with a 5 mm BBO BB-1H probe with z-gradients. Acquisition is performed using a CentOS workstation with Bruker TopSpin 2.1 software. The instrument is equipped with a 54-positions autosampler.
  • Bruker Avance III HD 400 console: Bruker AscendTM 400 magnet, equipped with a 5 mm PABBO BB/19F-1H/D probe with z-gradients and ATM accessory for Automatic Tuning and Matching. A 5 mm BBI 1H/D-BB probe with z-gradients is available as well. Acquisition is performed using a CentOS workstation with Bruker TopSpin 3.6.1 software. The instrument is equipped with a 24-positions autosampler and Bruker Autocalibrate function.
  • Bruker Avance II+ HD 600 console: Bruker 600 UltraShieldTM magnet and a CentOS workstation with Bruker TopSpin 3.6.1 software. 

 

Available probes:

 

  • 5 mm PABBO BB (31P-109Ag)-1H/D probe with z-gradients and ATM accessory for Automatic Tuning and Matching
  • 10 mm PABBO BB (31P-109Ag)-1H/D probe with z-gradients and ATM accessory for Automatic Tuning and Matching 
  • 10 mm PABBO BBLR (41K-109Ag)-1H/D custom probe with z-gradients and ATM accessory for Automatic Tuning and Matching. BB range shifted upwards as to include 97Mo, 89Y and 183W. 
  • 5 mm SEF 19F-1H/D probe, optimized for 19F observation with 1H decoupling.
  • 1 mm PATXI 1H/D-13C/15N probe with z-gradients and ATM accessory for Automatic Tuning and Matching
  • 5 mm PATXI 600S3 H-C/N-D probe with z-gradients and ATM accessory for Automatic Tuning and Matching 
  • 5 mm PABBI 1H/D-BB (31P-109Ag) probe with z-gradients and ATM accessory for Automatic Tuning and Matching 
  • 5 mm SEX 13C-1H/D probe, optimized for temperature ranges of -150 °C to 600 °C 
  • 4 mm HRMAS 1H/13C/15N/2H probe with 1H/13C/15N observe or decoupling channels and Magic Angle-gradient

Welcome to SOLVOMET

SOLVOMET is KU Leuven’s Centre for Solvometallurgy. SOLVOMET’s mission is to support its industrial and RTD partners in the conceptual and practical development of more sustainable solvometallurgical separation processes and new mining chemicals, which are subsequently tested using state-of-the-art lab-scale and mini pilot-scale experimental facilities.

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