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Nuclear magnetic resonance (NMR) spectroscopy

(1) Bruker Avance 300 MHz spectrometer: 1H, 13C 1D NMR, lab 00.422

(2) Bruker Avance III HD 400 spectrometer:  1H, 7Li, 11B, 13C, 19F, 27Al, 29Si, 31P, 51V 1D NMR, 1H–1H and 1H–13C 2D NMR, lab 00.422

(3) Bruker Avance II+ HD 600 MHz spectrometer: all NMR-sensitive nuclei, lab 00.421

The NMR Core facilities comprise a high-throughput area intended for daily use (Bruker Advance 300 and Bruker Avance III HD 400 spectrometer) and a research area, dedicated to specialized NMR experiments (Bruker Avance II+ 600 spectrometer).

 

Specifications:

 

  • Bruker Avance 300 console: Bruker 300 UltraShieldTM magnet, equipped with a 5 mm BBO BB-1H probe with z-gradients. Acquisition is performed using a CentOS workstation with Bruker TopSpin 2.1 software. The instrument is equipped with a 54-positions autosampler.
  • Bruker Avance III HD 400 console: Bruker AscendTM 400 magnet, equipped with a 5 mm PABBO BB/19F-1H/D probe with z-gradients and ATM accessory for Automatic Tuning and Matching. A 5 mm BBI 1H/D-BB probe with z-gradients is available as well. Acquisition is performed using a CentOS workstation with Bruker TopSpin 3.6.1 software. The instrument is equipped with a 24-positions autosampler and Bruker Autocalibrate function.
  • Bruker Avance II+ HD 600 console: Bruker 600 UltraShieldTM magnet and a CentOS workstation with Bruker TopSpin 3.6.1 software. 

 

Available probes:

 

  • 5 mm PABBO BB (31P-109Ag)-1H/D probe with z-gradients and ATM accessory for Automatic Tuning and Matching
  • 10 mm PABBO BB (31P-109Ag)-1H/D probe with z-gradients and ATM accessory for Automatic Tuning and Matching 
  • 10 mm PABBO BBLR (41K-109Ag)-1H/D custom probe with z-gradients and ATM accessory for Automatic Tuning and Matching. BB range shifted upwards as to include 97Mo, 89Y and 183W. 
  • 5 mm SEF 19F-1H/D probe, optimized for 19F observation with 1H decoupling.
  • 1 mm PATXI 1H/D-13C/15N probe with z-gradients and ATM accessory for Automatic Tuning and Matching
  • 5 mm PATXI 600S3 H-C/N-D probe with z-gradients and ATM accessory for Automatic Tuning and Matching 
  • 5 mm PABBI 1H/D-BB (31P-109Ag) probe with z-gradients and ATM accessory for Automatic Tuning and Matching 
  • 5 mm SEX 13C-1H/D probe, optimized for temperature ranges of -150 °C to 600 °C 
  • 4 mm HRMAS 1H/13C/15N/2H probe with 1H/13C/15N observe or decoupling channels and Magic Angle-gradient

Welcome to SOLVOMET ISC

SOLVOMET ISC is KU Leuven’s Industrial Service Centre for Circular Hydrometallurgy. We support mining, metallurgical & recycling companies in the development of more sustainable (circular, low-energy input) hydrometallurgical processes, using state-of-the-art lab & mini-pilot scale experimental facilities.

Corporate Presentation

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